X-ray structure analysis

Research group at Department of Condensed Matter Physics

Equipment of the X-ray laboratories

The instruments operated by members of our group include:

 

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Rigaku SmartLab with rotating anode

  • Source: copper rotating anode, 9 kW
  • Detectors: scintillation, linear, single-photon counting two-dimensional detector
  • Methods: diffraction, reflectivity, GID, (GI)SAXS, ...
  • Environments: ambient conditions; high-temperature dome chamber (up to 1100 °C)

The instrument is part of the CEITEC Nano core facility.

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Rigaku SmartLab for thin films (F-type)

  • Source: copper sealed anode, 3 kW
  • Detectors: scintillation, linear, single-photon counting two-dimensional detector
  • Methods: diffraction, reflectivity, GID, SAXS, ...

The instrument is part of the CEPLANT centre.

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Setup for X-ray diffraction with high collimation

  • Cu or Mo X-ray tube with parabolic graded mirror
  • Bartels type four-bounce channel-cut monochromator
  • Goniometer by Delong Instruments
  • Scintillation detector
  • Self-made software for driving the experiment

 

 

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Setup for X-ray reflectometry and diffraction with an annealing chamber

  • Cu X-ray tube with parabolic graded mirror
  • Goniometer by Delong Instruments
  • Temperature chamber for sample with a furnace (max 800 °C)
  • Scintillation detector
  • Self-made software for driving the experiment

 

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Setup for X-ray reflectometry and diffraction with high flux for ultra thin layers

  • Cu X-ray tube with parabolic graded mirror
  • Channel cut monochromator possibility
  • Goniometer by Huber
  • High temperature chamber for sample (max 1100 °C)
  • Scintillation detector
  • Self-made software for driving the experiment

 

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School X-ray source and goniometer PHYWE

  • Cu, Mo and W X-ray tubes
  • Measurement of X-ray tube spectra
  • Monocrystal orientation (lauegram)
  • X-ray fluorescence with an energy dispersive detector
  • Radiography

 

Other equipment we use:

  • Deposition: Langmuir-Blodgett trough
  • Deposition: Spin-coating
  • Sample preparation: clean room facility, chemical laboratory

 

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